Crystal structure of (N,N′-bis(2-(((2,6-diisopropylphenyl)imino)methyl)phenyl)benzene-1,2-diamido-κ4O,O′,O′′,O′′′)oxidovanadium(IV), C44H48N4OV

SYNTHESIS AND CRYSTAL STRUCTURE OF [PPh ] [WOS (CUNCS) ]

The reaction of [PPhJ, NOS,] with CuCl and KSCN (1 :3:3) in acetone produces the yell-ow crystals of [PPh,], [WOS,(CuNCS),]. The crystals are triclinic, space group P1(2), z=2, a=12.4823(7), b=12.9224(7), c=18.6395(10)?, ?=83.907(5), ?= 73.152(4), Y= 65.194(4)'. The crystal structure was determined by single crystal Xray diffraction methods (Mo-K ?) and refined by least-squares calculations ...

High-resolution crystal structure of the catalytic domain of human dual-specificity phosphatase 26.

Dual-specificity phosphatases (DUSPs) play an important role in regulating cellular signalling pathways governing cell growth, differentiation and apoptosis. Human DUSP26 inhibits the apoptosis of cancer cells by dephosphorylating substrates such as p38 and p53. High-resolution crystal structures of the DUSP26 catalytic domain (DUSP26-C) and its C152S mutant [DUSP26-C (C152S)] have been determi...

College Voice Vol. 26 No. 12

Crystal Structure of Nonaaquayttrium(III) Bromate at 100 K

The structure of the nonaaquayttrium (III) bromate, [Y(H2O)9](BrO3)3, at low temperature (100 K) has been studied by means of single-crystal X-ray diffraction. Crystallography shows a hexagonal unit cell, space group P63/mmc (No. 194) with Z = 2, a = b = 11.7104(11) Å, c = 6.6259(5) Å and V = 786.90(12) Å3 at 100 K. The hydra...

PREPARATION AND CRYSTAL STRUCTURE OF CaCl .[OC(NH ) ]

Calcium dichloride tetra urea was prepared by the reaction of calcium chloride with urea in aqueous solution. The crystals are monoclinic, a= 7.633, b= 12.45 1, c= 8.118 ?,? = 113.17, Z = 4, space group P 2,/a. The crystal structure was determined by single crystal X-ray methods and refined to R= 0.041. The calcium atoms are coordinated to four oxygen atoms of urea and to two chloride ions....